A number of modifications
to the original bent strip test method, mentioned earlier,
found their way into the research laboratory over the
years(2). Other methods were also developed. The spiral
contractometer was invented by Brenner and Senderoff(3)
in 1949, Kushner's stresometer(4) - in 1954. In 1958
the length-change (dilatometric) stress determination
method was proposed by Popereka(5.) An electronic strain
gauge apparatus6 constituting a modification of the stresometer
concept was patented in 1985. All of these as well as
the more recent optical (laser and interferometric) techniques
have been used for laboratory studies of stress during
electro- and electroless deposition.
For a test method
to be accepted and routinely used in an industrial
environment, as opposed to a research laboratory,
a number of fairly stringent additional requirements
need to be met. First and foremost, the test has to be
fast,
simple to use and interpret, the equipment - reliable
and robust, the results - accurate, repeatable and meaningful.
In the case of electroforming it also means, for reasons
to be discussed later, that stress tests must be performed
directly in plating tanks in a non- or minimally invasive
fashion. This last requirement simply means that carrying
out a stress test should not significantly alter the
established
electrochemical or hydrodynamic patterns in the process
tank. The ability to take measurements continuously and
ease of automation are also desirable features for an
industrial stress measurement method.
Most of the known
today stress testing methods fail to meet at least
one of these requirements and, therefore,
are suited more for laboratory than for industrial
use. So, the spiral contractometer is bulky, requires
calibration
prior to each test and deposit stripping afterwards.
The two disk membrane devices - the stresometer and
its electronic
modification are fairly complicated yet not sensitive
enough in the low stress level region (1,000 psi) and
require
periodic deposit stripping, too. The same is true about
the dilatometric stress measurement method, whose accuracy
is additionally affected by temperature variations.
The nature of electroforming itself dictates that of
most practical interest to the process engineer should
be low
stress levels which, as noted earlier, cause the least
distortion in the electroform. With this in mind, the
simplest yet sensitive enough measurement technique
for industrial
applications is still the bent strip method. One of
it's present commercial versions(7) utilizes disposable
brass
two-legged strips whose opposite sides are plated and
the resulting leg deflection caused by deposit stress
is measured
on a simple scale (Fig. 2). |